https://ogma.newcastle.edu.au/vital/access/ /manager/Index ${session.getAttribute("locale")} 5 https://ogma.newcastle.edu.au/vital/access/ /manager/Repository/uon:26983 15 ions cm⁻². The evolution of microstructure and induced defects of the irradiated sample with different doses was surveyed by combining grazing incident X-ray diffraction (GIXRD) using synchrotron radiation and variable energy positron beam analysis (PBA). With increasing irradiation dose, the crystallinity degrades gradually and leads to a combination of damaged Ti₃SiC₂ in combination with the precipitation of a TiCₓ phase. For high dose irradiation, a nano-dispersed TiCₓ phase becomes the dominant component. The PBA measurements indicate the formation of a new large vacancy-type defect that could be a cluster or void. The combination of GIXRD and PBA demonstrates that the damage of the MAX phase is more serious in the first 10 nm surface layer than that in the deeper layers closer to the final resting position of the projectile in the solid. The possible damage mechanisms have been discussed.]]> Sat 24 Mar 2018 07:26:59 AEDT ]]> https://ogma.newcastle.edu.au/vital/access/ /manager/Repository/uon:22092 0.67. It was found that a TiC nanocrystalline phase was formed under the high dose irradiation. However, a complete decomposition by irradiation did not take place even at 10.3 dpa. Post irradiation annealing to temperatures of 500–800 °C results in crystal regrowth of Ti₃SiC₂ and TiC phases.]]> Sat 24 Mar 2018 07:15:15 AEDT ]]>